Organic Structures from Spectra. H. L. Li

      

      Table of Contents

      1  COVER

      2  PREFACE

      3  LIST OF TABLES

      4  LIST OF FIGURES

      5  1 INTRODUCTION 1.1 GENERAL PRINCIPLES OF ABSORPTION SPECTROSCOPY 1.2 CHROMOPHORES 1.3 DEGREE OF UNSATURATION 1.4 CONNECTIVITY 1.5 SENSITIVITY 1.6 PRACTICAL CONSIDERATIONS

      6  2 ULTRAVIOLET (UV) SPECTROSCOPY 2.1 THE NATURE OF ULTRAVIOLET SPECTROSCOPY 2.2 BASIC INSTRUMENTATION 2.3 QUANTITATIVE ASPECTS OF ULTRAVIOLET SPECTROSCOPY 2.4 CLASSIFICATION OF UV ABSORPTION BANDS 2.5 SPECIAL TERMS IN UV SPECTROSCOPY 2.6 IMPORTANT UV CHROMOPHORES 2.7 THE EFFECT OF SOLVENTS

      7  3 INFRARED (IR) SPECTROSCOPY 3.1 ABSORPTION RANGE AND THE NATURE OF IR ABSORPTION 3.4 IMPORTANT IR CHROMOPHORES

      8  4 MASS SPECTROMETRY 4.1 IONISATION PROCESSES 4.2 INSTRUMENTATION 4.3 MASS SPECTRAL DATA 4.4 REPRESENTATION OF FRAGMENTATION PROCESSES 4.5 FACTORS GOVERNING FRAGMENTATION PROCESSES 4.6 EXAMPLES OF COMMON TYPES OF FRAGMENTATION

      9  5 ¹H NUCLEAR MAGNETIC RESONANCE (NMR) SPECTROSCOPY 5.1 THE PHYSICS OF NUCLEAR SPINS AND NMR INSTRUMENTS 5.2 BASIC NMR INSTRUMENTATION AND THE NMR EXPERIMENT 5.3 CHEMICAL SHIFTS IN 1H NMR SPECTROSCOPY 5.4 SPIN–SPIN COUPLING IN 1H NMR SPECTROSCOPY 5.5 ANALYSIS OF 1H NMR SPECTRA 5.6 CORRELATION OF 1H–1H COUPLING WITH STRUCTURE 5.7 THE NUCLEAR OVERHAUSER EFFECT (NOE) IN 1H NMR SPECTROSCOPY 5.8 LABILE AND EXCHANGEABLE PROTONS REFERENCES

      10  6 ¹³C NMR SPECTROSCOPY 6.1 COUPLING AND DECOUPLING IN ¹³C NMR SPECTRA 6.2 THE NUCLEAR OVERHAUSER EFFECT (NOE) IN 13C NMR SPECTROSCOPY 6.3 DETERMINING 13C SIGNAL MULTIPLICITY USING DEPT 6.4 SHIELDING AND CHARACTERISTIC CHEMICAL SHIFTS IN 13C NMR SPECTRA

      11  7 2-DIMENSIONAL NMR SPECTROSCOPY 7.1 PROTON–PROTON INTERACTIONS BY 2D NMR 7.2 PROTON–CARBON INTERACTIONS BY 2D NMR

      12  8 MISCELLANEOUS TOPICS 8.1 SOLVENTS FOR NMR SPECTROSCOPY 8.2 SOLVENT-INDUCED SHIFTS 8.3 DYNAMIC NMR SPECTROSCOPY – THE NMR TIME-SCALE 8.4 THE EFFECT OF CHIRALITY 8.5 THE NMR SPECTRA OF “OTHER NUCLEI”

      13  9 DETERMINING THE STRUCTURE OF ORGANIC COMPOUNDS FROM SPECTRA Collection of Spectra 9.1 SOLVING PROBLEMS 9.2 WORKED EXAMPLES

      14  10 PROBLEMS Problem 1 Problem 2 Problem 3 Problem 4 Problem 5 Problem 6 Problem 7 Problem 8 Problem 9 Problem 10 Problem 11 Problem 12 Problem 13 Problem 14 Problem 15