Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy – an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
A unique approach to teaching particle and rigid body dynamics using solved illustrative examples and exercises to encourage self-learning The study of particle and rigid body dynamics is a fundamental part of curricula for students pursuing graduate degrees in areas involving dynamics and control of systems. These include physics, robotics, nonlinear dynamics, aerospace, celestial mechanics and automotive engineering, among others. While the field of particle and rigid body dynamics has not evolved significantly over the past seven decades, neither have approaches to teaching this complex subject. This book fills the void in the academic literature by providing a uniquely stimulating, “flipped classroom” approach to teaching particle and rigid body dynamics which was developed, tested and refined by the author and his colleagues over the course of many years of instruction at both the graduate and undergraduate levels. Complete with numerous solved illustrative examples and exercises to encourage self-learning in a flipped-classroom environment, Dynamics of Particles and Rigid Bodies: A Self-Learning Approach: Provides detailed, easy-to-understand explanations of concepts and mathematical derivations Includes numerous flipped-classroom exercises carefully designed to help students comprehend the material covered without actually solving the problem for them Features an extensive chapter on electromechanical modelling of systems involving particle and rigid body motion Provides examples from the state-of-the-art research on sensing, actuation, and energy harvesting mechanisms Offers access to a companion website featuring additional exercises, worked problems, diagrams and a solutions manual Ideal as a textbook for classes in dynamics and controls courses, Dynamics of Particles and Rigid Bodies: A Self-Learning Approach is a godsend for students pursuing advanced engineering degrees who need to master this complex subject. It will also serve as a handy reference for professional engineers across an array of industrial domains.
Covers all the aspects of the recent achievements in silver catalyzed reactions Silver catalysis has emerged as a powerful tool in the field of organic synthesis. This comprehensive book systematically explores the unique performance of silver catalysis, introducing all the recent progress of silver catalysis in organic synthesis. It clearly emphasizes the unique features of silver catalysis and provides the reaction mechanism involved. This two-volume book also provides vivid schematics and tables throughout to enhance the accessibility to the relevant theory and mechanisms. Silver Catalysis in Organic Synthesis begins with an introduction to Silver Chemistry before moving on to chapters covering: Silver-Catalyzed Cycloaddition Reactions; Silver-Catalyzed Cyclizations; Silver-Mediated Radical Reactions; Silver-Mediated Fluorination, Perfluoroalkylation and Trifluoromethylthiolation Reactions; Coupling Reactions and C-H Functionalization; Silver-Catalyzed CO2 Incorporation; Silver-Catalyzed Carbene, Nitrene, and Silylene Transfer Reactions; Asymmetric Silver-Catalyzed Reactions; Silver-Catalyzed Reduction and Oxidation of Aldehydes and Their Derivatives; Silver Complexes in Organic Transformations; and Silver Nanoparticles in Organic Transformations. -Covers recently developed organic reactions catalyzed by silver, along with their reaction mechanism -Introduces many new reactions and mechanisms related to silver catalysis -Offers professionals and newcomers in the related fields a survey of new advances in silver catalysis in organic synthesis Silver Catalysis in Organic Synthesis will appeal to a wide readership including chemists, biochemists, pharmaceutical scientists, biomedical researchers, agriculture scientists, and graduate students in the related fields.
An informative look at the theory, computer implementation, and application of the scaled boundary finite element method This reliable resource, complete with MATLAB, is an easy-to-understand introduction to the fundamental principles of the scaled boundary finite element method. It establishes the theory of the scaled boundary finite element method systematically as a general numerical procedure, providing the reader with a sound knowledge to expand the applications of this method to a broader scope. The book also presents the applications of the scaled boundary finite element to illustrate its salient features and potentials. The Scaled Boundary Finite Element Method: Introduction to Theory and Implementation covers the static and dynamic stress analysis of solids in two and three dimensions. The relevant concepts, theory and modelling issues of the scaled boundary finite element method are discussed and the unique features of the method are highlighted. The applications in computational fracture mechanics are detailed with numerical examples. A unified mesh generation procedure based on quadtree/octree algorithm is described. It also presents examples of fully automatic stress analysis of geometric models in NURBS, STL and digital images. Written in lucid and easy to understand language by the co-inventor of the scaled boundary element method Provides MATLAB as an integral part of the book with the code cross-referenced in the text and the use of the code illustrated by examples Presents new developments in the scaled boundary finite element method with illustrative examples so that readers can appreciate the significant features and potentials of this novel method—especially in emerging technologies such as 3D printing, virtual reality, and digital image-based analysis The Scaled Boundary Finite Element Method: Introduction to Theory and Implementation is an ideal book for researchers, software developers, numerical analysts, and postgraduate students in many fields of engineering and science.
Completely revised and updated, the third edition of this bestseller discusses the concept and ongoing development of using methanol as a transportation fuel, energy storage medium, and as a raw material to replace oil. The contents have been expanded by 35% with new chapters on energy storage, methanol from biomass and waste products, as well as on carbon dioxide recycling. Written by the late Nobel laureate George Olah and his team, this is an inspiring read for anyone concerned with the major challenge posed by tomorrow's energy and environmental problems.
This richly illustrated hands-on guide is designed for researchers, teachers and practitioners. The huge selection of examples taken from science, basic teaching of physics, practical applications in industry and a variety of other disciplines spanning the range from medicine to volcano research allows readers to pick those that come closest to their own individual task at hand. Following a look at the fundamentals of IR thermal imaging, properties of the imaging systems, as well as basic and advanced methods, the book goes on to discuss IR imaging applications in teaching, research and industry. Specific examples include thermography of buildings, microsystems and the rather new field of IR imaging of gases. Impartially written by expert authors in the field from a renowned applied science institution, who are in the unique position of having both experience in public and private research and in teaching, this comprehensive book can be used for teaching beginners in the field as well as providing further education to specialized staff, students and researchers.
Provides a complete understanding of how our bodies respond to toxicants, and the principles used to assess the health risks of specific exposure scenarios Toxicology and Risk Assessment: A Comprehensive Introduction, Second Edition reflects recent advances in science and technology, and provides the scientific background and methodological issues to enable the reader to understand the basic principles in toxicology and to evaluate the health risks of specific exposure scenarios. Completely updated with the latest information, this book offers a concise introduction to the subject. It is divided into five sections: Principles in Toxicology, Organ Toxicology, Methods in Toxicology, Regulatory Toxicology, and Specific Toxicity. The 2nd Edition adds new chapters that cover recent scientific and technological advances and current topics including the endocrine system, alternatives to animal testing, risk assessment and thresholds for carcinogens, European and international regulation, nanomaterials, fuels, fragrances, and agrochemicals. Concentrates on the basic concepts of toxicology and provides sufficient information for the reader to become familiar with them in order to understand the principles and to evaluate the risks at given exposures 30% new chapters cover recent scientific and technological advances including alternatives to animal testing; genotoxic carcinogens; REACH regulations; nanomaterials; fuels; fragrances; PAHs; and agrochemicals Written by a team of international specialists, and edited by two outstanding scientists in the field Fully updated and expanded, Toxicology and Risk Assessment: A Comprehensive Introduction, Second Edition is an essential text for any student or researcher with an interest in toxicology and related risk assessments.
Engage students in mathematics using growth mindset techniques The most challenging parts of teaching mathematics are engaging students and helping them understand the connections between mathematics concepts. In this volume, you'll find a collection of low floor, high ceiling tasks that will help you do just that, by looking at the big ideas at the third-grade level through visualization, play, and investigation. During their work with tens of thousands of teachers, authors Jo Boaler, Jen Munson, and Cathy Williams heard the same message—that they want to incorporate more brain science into their math instruction, but they need guidance in the techniques that work best to get across the concepts they needed to teach. So the authors designed Mindset Mathematics around the principle of active student engagement, with tasks that reflect the latest brain science on learning. Open, creative, and visual math tasks have been shown to improve student test scores, and more importantly change their relationship with mathematics and start believing in their own potential. The tasks in Mindset Mathematics reflect the lessons from brain science that: There is no such thing as a math person – anyone can learn mathematics to high levels. Mistakes, struggle and challenge are the most important times for brain growth. Speed is unimportant in mathematics. Mathematics is a visual and beautiful subject, and our brains want to think visually about mathematics. With engaging questions, open-ended tasks, and four-color visuals that will help kids get excited about mathematics, Mindset Mathematics is organized around nine big ideas which emphasize the connections within the Common Core State Standards (CCSS) and can be used with any current curriculum.
В монографии описываются новые манипулятивные практики, которые предлагается рассмотреть в социологическом дискурсе. Отдельно рассматриваются манипуляции и манипулятивные стратегии в политической сфере, противодействие им и возможность встречных манипулятивных действий. При описании новых манипулятивных техник в центре внимания оказываются интернет-технологии, их использование в целях влияния на массы. Издание адресовано научным работникам, преподавателям, аспирантам и студентам, всем, кто интересуется проблемами социального манипулирования, социального влияния и в целом власти-подчинения.